
Luminescence dating of reticulated red clay buried in Lanshanmiao Paleolithic site in Zhejiang Province, southern China
LU Ying, SUN Xuefeng, XU Xinmin, LIU Yalin, YI Shuangwen
Journal of Geographical Sciences ›› 2020, Vol. 30 ›› Issue (9) : 1436-1450.
Luminescence dating of reticulated red clay buried in Lanshanmiao Paleolithic site in Zhejiang Province, southern China
The Lanshanmiao (LSM) Palaeolithic site, which was excavated in the summer of 2017 by the Zhejiang Provincial Institute of Cultural Relics and Archaeology, is the only excavated palaeolithic site in central Zhejiang Province to date. Luminescence dating methods, including optical stimulated luminescence (OSL) and thermal transfer OSL (TT-OSL) for quartz and post-infrared (IR) stimulated luminescence (pIRIR290) for feldspar, were used to determine the age of the LSM site. The results showed that the LSM section developed before 145.5 ± 12.5 ka and ended after 17.1 ± 1.0 ka. The TT-OSL dating of samples NJU2576 and NJU2615 showed that palaeolithic artifact-bearing layer was between 150 and 100 ka in age. The age range of the palaeolithic layer mainly corresponded to the transition between Marine Isotope Stage (MIS) 6 and MIS5. Our study showed that hominins prominently occupied the LSM site during the glacial and interglacial stages, when it exhibited a floodplain environment.
Lanshanmiao site / Palaeolithic / reticulated red clay / luminescence dating / glacial / interglacial {{custom_keyword}} /
Figure 1 Locations of the LSM (9), Qiliting (QLT) (5), and Yindinggang (YDG) (3) sites and other areas in the Zhejiang Province, including 1-Zijinshan, 2-Hexi Cave No. 1, 4-Wangjiashan, 6-Shangmakan, 7-Tonglu Man, and 8-Jiande Man |
Figure 5 Curves of the magnetic susceptibility, radiation dose (U, Th, and K), and water content |
Lab No. | Depth (m) | wc (%) | U (ppm) | Th (ppm) | K (%) | Dose rate (Gy/ka) | De (Gy) | Age (ka) | |||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|
OSL & TT | pIRIR290 | OSL | TT-OSL | pIRIR290 | OSL | TT-OSL | pIRIR290 | ||||||
NJU2572 | 0.10 | 18.2 | 2.88±0.11 | 14.1±0.38 | 0.87±0.04 | 2.44±0.11 | - | 41.7±1.4 | 47.0±7.6 | - | 17.1±1.0 | 19.9±3.4 | - |
NJU2574 | 0.75 | 18.0 | 2.67±0.10 | 13.6±0.38 | 0.86±0.04 | 2.30±0.11 | - | >217 | 222.5±4.8 | - | >94 | 96.8±5.4 | - |
NJU2576 | 1.45 | 16.3 | 2.89±0.11 | 14.4±0.39 | 0.88±0.04 | 2.42±0.12 | - | - | 291.4±39.4 | - | - | 120.3±17.5 | - |
NJU2577 | 1.75 | 14.6 | 3.21±0.12 | 14.7±0.40 | 0.82±0.04 | 2.48±0.12 | - | - | 311.1±45.1 | - | - | 125.6±19.4 | - |
NJU2578 | 2.75 | 15.6 | 3.44±0.12 | 15.7±0.42 | 1.03±0.04 | 2.73±0.13 | 3.20±0.13 | >331 | 346.7±17.3 | 376±14 | >121 | 126.9±9.3 | 118±7 |
NJU2615 | 4.00 | 18.6 | 3.36±0.13 | 14.9±0.42 | 0.91±0.04 | 2.47±0.12 | 3.00±0.12 | - | 358.7±24.6 | 412±42 | - | 145.5±12.5 | 167±18 |
* “>” means saturated age estimation; “wc” = water content |
Figure 6 The LSM section, ages, and the cultural layer correspondence to marine oxygen isotopic stages |
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AbstractA single-aliquot dating procedure for measuring the equivalent dose in fine-grained quartz extracted from Chinese loess has been developed and tested. The optically stimulated luminescence (OSL) signal used for construction of the dose–response curve is termed the recuperated OSL (ReOSL) signal; it is the difference between the thermally transferred OSL signal measured after heating to {{custom_citation.content}}
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The present study focuses on the stratigraphy of two Late Quaternary boreholes that are primarily composed of fine-grained sediments. Analyses of the two boreholes include OSL and U-series dating, pollen and microfossils, tending to reconstruct the high resolution climatic stratigraphy, and therefore to define the chronostratigraphy of the Late Quaternary. It is also our aim to discuss the two transgressions and their mechanisms during that period. Results demonstrate that climate fluctuations recorded by the two boreholes correspond to the marine oxygen isotope stages(MIS). Thick layer of coarser grained fluvial deposits and the third layer of “hard mud” were deposited in the study area during MIS 6, reflecting a cold climate. The sediments became fine-grained and indicate a coastal marsh depositional environment during MIS 5. The second layer of “hard mud” was deposited during MIS 4. Fine-grained coastal marsh deposits dominated in the study area during early MIS 3, while lagoon-beach ridges prevailed during middle and late MIS 3, forming a layer of silt and fine sand in the coastal plain. The MIS 2 strata are composed of a typical sedimentary sequence with coarse grain in the lower section and fine grain in the upper section, i.e. yellowish grey or brownish yellow silt and brownish yellow or dark green “hard mud”,respectively. The three “hard mud” layers of MIS 6, MIS 4 and MIS 2 are the marker beds in the upper Quaternary in the Changjiang delta area. Marine incursions occurred during both MIS 5 and MIS 3. Higher topography and abundant freshwater and terrigenous material inputs determined that the marine influence during MIS 5 was weak. By contrast, the lagoon-beach ridges environment lack of freshwater supply led to the formation of the widely developed transgressive strata of middle and late MIS 3.
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Kind of red, loose or semi-cemented sediment was widely distributed in tropical and subtropical regions of China, called Quaternary Red Clay (QRC). The causes and definitions of QRC were argued intensely. Depends on matrix, the QRC can be broadly divided into two types, Sedimentary Red Clay (SRC) and Laterite Weathering Crust (LWC). The SRC, development on all kinds of Quaternary sediments, always got similar profile configuration. The layer of SRC profile, from top to bottom, was Homogeneous Red Clay (HRC) or Yellow- Brown Earth (YBE), Vermicular Red Clay (VRC) and weathered gravel or bedrock; LWC was a kind of residual soil, formed by different types of bedrock weathering and widely distributed in tropical and subtropical regions. Representative LWC profile was generally contained weathered red soil, semi-weathered layer and bedrock. In this article, magnetic characteristics of basalt and granite weathering crust in Xinchang, Zhejiang Province, Quaternary SRC in Nanchang, Jiangxi Province were analyzed. The main characteristics of LWC are that, magnetic characteristics distinction of two kinds of weathering crust in the same climate zone was relatively large and the magnetic characteristics were determined by the matrix; Magnetisability of basalt weathering crust increased after a small decrease with the increasing weathering intensity; Magnetisability of granite weathering crust increased with increasing weathering intensity. Intense weathering made mineral particles tapering and antiferromagnetic minerals reduce in these two kinds of weathering crust. The main characteristics of sedimentary red clay were that, magnetisability of HRC was greater than VRC at least one order of magnitude. The content of antiferromagnetic mineral in VRC was much greater than the HRC. The content of Pseudo- Single Domain and Multidomain grain in VRC was much greater than the HRC. The magnetic characteristics change rule in SRC did not meet with the weathering rule prove that maybe HRC and VRC got different provenance in Quaternary sedimentary red clay profile.
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The Xiaogushan cave site is one of the most important prehistoric sites in North China. The stone and bone artifacts found in the cave are similar to European contemporaneous artifacts. Cave deposits consist of five layers that have been dated from 46,353 +/- 1179 to 4229 +/- 135 cal. yr BP, using radiocarbon dating techniques on charcoal and bone samples collected from Layers 2-5. In this paper, optically stimulated luminescence (OSL) techniques were applied to date six samples taken from Layers 1-3. The luminescence properties of the fine-grained and coarse-grained quartz extracts indicate that the materials are suitable for OSL dating using a single-aliquot regeneration-dose (SAR) protocol. The OSL ages obtained are broadly consistent with the stratigraphy and the associated calibrated radiocarbon ages. The dating results show that the cave was first occupied by humans about 70 ka. The human occupation of the cave may be related to climate change. An occupation hiatus is inferred to between approximately 17 to approximately 10 ka. The stone and bone artifacts found in Layers 2 and 3 may indicate the Middle to Upper Paleolithic transitions in the region.
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We thank Zeng Qiongxuan, Xu Xinghua, and Lu Yiming for their assistance.
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